Table Of Content

National Nanotechnology Infrastructure Network Research Experience for Undergraduates (NNIN REU) Program International Research Experience for Graduates (NNIN iREG) Program International Research Experience for Undergraduates (NNIN iREU) Program 2013 Research Accomplishments ©2013 Silicon Nanophotonic Add-Drop Filter Based on High-Q Square Resonant Cavities; Emily Donahue, pages 174-175 Deposition of the Immobilization Layer 3-Aminopropyltriethoxysilane on GaN for Extremo- phile-Based Biosensors; Tiffany Huang, pages 218-219 Understanding Magnetic Plasmon Mode Mixing Using Electron Energy Loss Spectroscopy; Harrison J. Goldwyn, pages 194-195 Determination of Strength Degrada- tion Mechanisms of Native Oxide on Silicon Nanostructures; Rafael Jesus Haro, pages 122-123 Conformable Conducting Polymer Electrodes used with an Ionic Liquid Gel for Electroencephalography; Developing Bioinspired Slippery Coating on Industrial Steels; Keiko Kato, pages 126-127 Camryn Johnson, pages 18-19 Synthesis and Covalent Attachment of {M4} Polynuclear Me- Curved Functionalized Micro fluidic Channels...; Azobenzene Functionalized DNA for Light-Induced DNA Stringency; tallic Complexes....; Christopher A. Nakamoto, pages 70-71 Ang Li, pages 32-33 Hannah Zeitler, pages 78-79 TOC&INTRO National Nanotechnology Infrastructure Network Research Experience for Undergraduates Program 2013 Research Accomplishments 2013 NNIN REU Reports by Research Focus; i-x The National Nanotechnology Infrastructure Network NNIN Director Welcome; xi (NNIN) is an integrated partnership of fourteen NNIN Sites & Corporate Sponsors; xii user facilities, supported by the National Science Foundation. NNIN provides opportunities for nano 2013 NNIN Interns, by Site; science and nanotechnology research, including support in fabrication, synthesis, characterization, modeling, Arizona State University; page xiv design, computation, and handson training in an open Cornell University; page xv environment. The NNIN members includes: Georgia Institute of Technology; page xvi Harvard University; page xvii • ASU NanoFab, Arizona State University Howard University; page xviii • Cornell NanoScale Facility, Cornell University The Pennsylvania State University; page xix • Nanotechnology Research Center, Georgia Institute of Technology Stanford University; page xx • Center for Nanoscale Systems, Harvard University University of California, Santa Barbara; page xxi • Howard Nanoscale Science and Engineering Facility, University of Colorado at Boulder; page xxii Howard University • Penn State Nanofabrication Facility, The University of Michigan, Ann Arbor; page xxiii The Pennsylvania State University University of Minnesota-Twin Cities; page xxiv • Stanford Nanofabrication Facility, Stanford University The University of Texas at Austin; page xxv • UCSB Nanofabrication Facility, University of California, Santa Barbara University of Washington; page xxvi • Colorado Nanofabrication Laboratory, Washington University in St. Louis; page xxvii University of Colorado, Boulder The 2013 NNIN iREG Program; page xxviii • Lurie Nanofabrication Facility, University of Michigan The 2013 NNIN iREU Program; page xxviii • Minnesota Nano Center, University of Minnesota • Microelectronics Research Center, Commonly Used Abbreviations The University of Texas at Austin & Their Meanings; xxix-xxxviii • NanoTech User Facility, University of Washington • Nano Research Facility, Washington University at St. Louis 2013 Research Accomplishments; pages 2-233 Index; pages 235-240 http://www.nnin.org/ •2013•NNIN•REU•RESEARCH•ACCOMPLISHMENTS• i TOC&INTRO Biological Applications, pages 2-57 Binding of DU145 Prostate Tumor Cancer Cells to Silicon Carbide ...........................................2 Ayobami Adeleke, Chemistry, Delaware State University . . . . . . . NNIN REU Site: Howard University Characterization of Polymer Films on Silicon Photonics Devices for Blood Analysis................ 4 Alexandra S. Benson, Chemistry, Hope College . . . . . . . . . . . NNIN REU Site: University of Washington Developing Nanoscale Electrodes for Sensitive Detection of Brain Cell Activities........................................................6 Dara Bobb-Semple, Chemistry, Stony Brook University . . . . . . . . . . . . . . . NNIN REU Site: Stanford University Delivery of Immunosuppressive DNA Drug for Treatment of Autoimmune Diseases....................................................8 Colin Burns-Heffner, Bioengineering, Clemson University . . . . . . . . . . . . . . . . NNIN iREU Site: NIMS, Japan Cisplatin-Based Metal Organic Framework Nanoparticles for Targeted Drug Delivery and Tumor Imaging .................10 Samantha Renee Corber, Physics, Chemistry, Washburn University . . . .NNIN REU Site: Washington University in St. Louis System Automation for High Throughput Biosensor................................................................................................12 Dakota Nevans Crisp, Physics and Engr. Physics, Southeast Missouri State University. . .NNIN REU Site: University of Texas Engineering Three-Dimensional Biological Scaffolds Using a Modified Rotary Jet Spinning System ..........................14 John Phillip Ferrier, Jr., Physics / Mathematics, University of Central Arkansas . . . . . NNIN REU Site: Harvard University Fabrication of Nanofluidic Devices for DNA Confinement .........................................................................................16 Suman Gunasekaran, Engineering Sciences, Harvard University . . . . NNIN REU Site: University of Minnesota-Twin Cities Conformable Conducting Polymer Electrodes used with an Ionic Liquid Gel for Electroencephalography ....................18 Camryn Johnson, Biological Engineering, Louisiana State University at Baton Rouge . . . . . . . .NNIN iREU Site: France Development of Microfluidic Devices for Use in Immunophenotyping....................................................................... 20 Meghan Kazanski, Biomedical Engineering, University of Rochester . . . .NNIN REU Site: University of Michigan, Ann Arbor Cell Polarization on Circular Topography with Various Radii of Curvature...............................................................22 Peter Kim, Material Science and Engineering, Northwestern University . . . . . . . NNIN REU Site: University of Washington Fabrication of “Barcode” Nanowires for Multiplexed Detection in Biological Assays................................................24 Seung Yeon Kim, Chemical and Biomolecular Engr., Georgia Institute of Technology . . NNIN REU Site: University of Minnesota ii •2013•NNIN•REU•RESEARCH•ACCOMPLISHMENTS• TOC&INTRO Effects of Cellular Architecture on MDA-MB-231 Breast Cancer Cell Motility .............................................................26 Ted Kocher, Biological Systems Engineering, University of Nebraska-Lincoln NNIN REU Site: University of Minnesota-Twin Cities Microfluidics for the Study of Breast Cancer ......................................................................................................... 28 Lisa Kriegh, Biosystems Engineering, Oklahoma State University . . . . . . . . . . NNIN REU Site: Arizona State University Design of Synthetic Protein Membranes Using Droplet Microfluidics ......................................................................30 Corey Landry, Biological Engineering, Louisiana State University . . . . . . . . . . .NNIN REU Site: Harvard University Curved Functionalized Microfluidic Channels for the Study of Cell Dynamics...........................................................32 Ang Li, Department of Biomedical Engineering, Georgia Institute of Technology. . . . . . . NNIN REU Site: Harvard University Identifying the Biomechanical Effects of UV Resistant Molecules and Nanoparticles on Human Skin........................34 Sarah Nainar, Biochemistry, Washington & Jefferson College . . . . . . . . . . . . . NNIN REU Site: Stanford University Fabrication of Nano Ion Pumps for Retinal and Neural Prosthesis...........................................................................36 Zachary Pritchard, Chemical and Biomolecular Engineering, Georgia Institute of Technology . . . . . NNIN REU Site: UCSB Differentiation of Human Mesenchymal Stem Cells to Schwann Cells on Electrospun Nanofibers..............................38 Shelby Pursley, Biological Engineering, Louisiana State University. . . . . . NNIN REU Site: Georgia Institute of Technology Electrohydrodynamic Jet Printing on Hydrogel Substrates for Cell Culturing Applications...................................... 40 Audre Ramey, Mechanical Engineering, University of Portland. . . . . . .NNIN REU Site: University of Michigan, Ann Arbor Surface Ligand Density Dependence of Collective Cell Migration on Photoactivatable Self Assembled Monolayers...42 Radu Reit, Biomedical Engineering, Georgia Institute of Technology . . . . . . . . . . . . . NNIN iREU Site: NIMS, Japan Micro-Scale Microbial Fuel Cell: Petroleum Biosensing........................................................................................... 44 Anne Showalter, Biological Chemistry, Culver-Stockton College . . . . . . . . . . NNIN REU Site: Arizona State University Dynamics of Bacterial Quorum Sensing in Microfluidic Devices .............................................................................. 46 Peter Youpeng Su, Chemical and Biomolecular Engineering, University of California, Berkeley NNIN REU Site: Georgia Tech Fabrication of Flexible, Implantable Probes for in vivo Recording of Neural Activity ................................................ 48 Brianna Thielen, Engineering, Harvey Mudd College . . . . . . . . . .NNIN iREU Site: Saint-Étienne et Gardanne, France The Study of Disposable Substrates in Surface Acoustic Wave Devices................................................................. 50 Christine Truong, Physics, Polytechnic Institute of New York University. . . NNIN REU Site: The Pennsylvania State University The Impact of MEMS-Produced Micro-Electrode Material Coating on Dental Plaque Biofilm Growth .........................52 Katherine Warthen, Bioengineering, Montana State University . . . . . .NNIN REU Site: University of Michigan, Ann Arbor •2013•NNIN•REU•RESEARCH•ACCOMPLISHMENTS• iii TOC&INTRO Fabrication of Microchemical Field-Effect Transistor ............................................................................................. 54 Ming-Lun Wu, Biomedical Engineering, University of Florida . . . . . .NNIN REU Site: University of Minnesota-Twin Cities Exploring the Effects of Theophylline on Neutrophil Function in Inflammatory Diseases .......................................... 56 Ashlyn Young, Biomedical Engineering, University of North Carolina at Chapel Hill . . NNIN REU Site: University of Minnesota Chemistry, pages 58-79 Use of Field-Induced Surface-Organometallic Interactions to Control Selectivity in Rh-Catalyzed Organic Reaction ..58 Dylan Barber, Chemistry Major, Williams College . . . . . . . . . . . NNIN REU Site: Stanford University Area-Selective Atomic Layer Deposition: New Recipe Development .................................................60 Tyler Erjavec, Physics, The Ohio State University . . . . . . . . . . . . NNIN REU Site: Cornell University Poly(3-alkyldithienothiophene): Synthesis, Structure and Optical Properties ....................62 Yuki Hamasaki, Applied Chemistry, Kyushu University, Japan . . . . . NNIN iREG Site: University of Washington Synthesis and Characterization of Functional Organic and Supramolecular Nanomaterials .................................... 64 Melinda Jue, Chemical Engineering, University of Texas at Austin . . . . . . . . . . . . . . NNIN iREU Site: NIMS, Japan Crumpled Graphene Oxide Nanostructures for Advanced Water Treatment Technologies........................................ 66 Christine Le, Biochemistry, Brown University . . . . . . . . . . . . . .NNIN REU Site: Washington University in St. Louis Direct Nano Patterning of Anisotropic Conjugated Polymer .................................................................................... 68 Azusa Miyagawa, Materials Science, Japan Advanced Institute of S&T . . . . . . . NNIN iREG Site: University of Michigan Synthesis and Covalent Attachment of {M4} Polynuclear Metallic Complexes to Oxidized Carbon Nanotubes...........70 Christopher A. Nakamoto, Chemistry, Beloit College . . . . . . . . . . . . . . . .NNIN iREU Site: Jülich, Germany Effects of Hydrophilic Membrane Modifications and Natural Organic Matter Fouling on Reverse Osmosis Membrane Performance.....................................................72 Justin Nauman, Chemical Engineering, Purdue University . . . . . . . .NNIN REU Site: Washington University in St. Louis iv •2013•NNIN•REU•RESEARCH•ACCOMPLISHMENTS• TOC&INTRO Controlled Self-Assembly of Metallated and Non-Metallated Peptidic Arrays............................................................74 Geoffrey Vrla, Chemistry, Middlebury College . . . . . . . . . . . . . . . . . . . . . NNIN iREU Site: NIMS, Japan Directed Self Assembly of Mixed Nanowire Populations via Lithographic Microwells...............................................76 Allison Wustrow, Chemistry, University of California Berkeley . . . . . . NNIN REU Site: The Pennsylvania State University Azobenzene Functionalized DNA for Light-Induced DNA Stringency .........................................................................78 Hannah Zeitler, Physical Chemistry, Whitworth University . . . . . . . . . . . NNIN REU Site: University of Washington Electronics, pages 80-101 Inkjet Printed Interconnects for Multilayer Flexible Electronics...................................80 J. Daniel Binion, Electrical Engineering, Grove City College . . . . . . NNIN REU Site: The University of Texas at Austin Investigation of Molybdenum Disulfide Transistors with Aluminum Oxide Passivation.....................................82 Marc Castro, Electrical Engr., University of Texas at San Antonio . . . NNIN REU Site: NASCENT, The University of Texas at Austin Fabrication of Accelerometers using Paper MEMS Substrates .............................................................................. 84 Marco De Lira, Mechanical and Energy Engineering, University of North Texas . . . . . . NNIN REU Site: Howard University Nanoscale High-Speed Transparent Electronics using E-Beam Patterning of Zinc Tin Oxide Thin Film Transistors.... 86 Andinet Desalegn, Material Science and Engineering, University of Maryland . . . . NNIN REU Site: University of Michigan Zinc Oxide Based Ultraviolet Solar Cells for Self-Powered Smart Window Application............................................ 88 Benjamin Helfrecht, Materials Engineering, Purdue University . . . . . . . . . .NNIN REU Site: Arizona State University Researching All-Aluminum n-Type Silicon Solar Cells.............................................................................................. 90 Tomoyuki Inoue, Electrical Engineering, the University of Tokyo . . . . . . . . . .NNIN iREG Site: Arizona State University Trap Density Analysis of High Dielectric Oxides on III-V Semiconductors..................................................................92 Daniel Loman, Physics, Siena College . . . . . . . . . . . . . . . NNIN REU Site: University of California, Santa Barbara Influence of Planar Organic Electrochemical Transistor Device Geometry in the Characterization of Barrier Tissue 94 Kaleigh Margita, Chemistry, Newberry College. . . . . . . . . . . . .NNIN iREU Site: Saint-Étienne et Gardanne, France •2013•NNIN•REU•RESEARCH•ACCOMPLISHMENTS• v TOC&INTRO Examining Metal/SnS Contact Resistances for the Increase of SnS Solar Cell Efficiency........................................ 96 Shay Goff Wallace, Materials Science and Engineering, University of Minnesota-Twin Cities NNIN REU Site: Harvard University Radio Frequency Switches Using Phase Change Materials..................................................................................... 98 Kosuke Wataya, Mechanical Engineering, Tohoku University, Sendai, Japan NNIN iREG Site: University of Michigan, Ann Arbor Fabrication and Characterization of InGaAs MOSCaps with HfO Dielectrics..........................................................100 2 Jill Wenderott, Physics, University of Kansas . . . . . . . . . . . . NNIN REU Site: University of California, Santa Barbara Materials, pages 102-161 Effect of Reactive Ion Etching on Laser-Annealed Low-k SiCOH Materials...................... 102 Kris Beykirch, Physics, Corning Community College . . . . . . . . . . NNIN REU Site: Cornell University Characterization of Single Component Molecular Glass Resists................................................. 104 Maike Blakely, Chemistry, Chatham University, Pittsburgh, PA . . . . . NNIN REU Site: Cornell University Silver Nanoplates; Structural Stability and Optical Properties...............................................................................106 Tyler Burkett, Chemical Engineering, University of Florida . . . . . . . . . NNIN REU Site: Georgia Institute of Technology Low-Temperature Cu Segregation and Oxidation in Microwaved Ag-Cu Alloys .........................................................108 Brandi T. Burton, Physics, Norfolk State University . . . . . . . . . . . . . . . NNIN REU Site: Arizona State University Development of Platinum Embedded in Reduced Graphene Oxide (Pt@rGO) for Fuel Cell Applications ......................110 Michelle Chen, Chemical Engineering, Cornell University . . . . . . . NNIN REU Site: University of California, Santa Barbara An Experimental and Theoretical Investigation of Ultrasound Transmission in Bubbly PDMS Phononic Crystals... ... .112 Caleb Christianson, Engineering Physics, University of Kansas . . . . . . . . . . . . NNIN REU Site: Cornell University Growth of Graphene on Various Substrates............................................................................................................114 Crystal T. Chukwurah, Biomedical Engineering, Duke University . . . . . . . . . . . NNIN REU Site: Howard University Investigation of Microfluidic Integration in Magneto-Nanosensor Based Protein Biomarker Detection ......................116 Stephanie Cone, Biomedical Engineering, University of Arkansas . . . . . . . . . . .NNIN REU Site: Stanford University vi •2013•NNIN•REU•RESEARCH•ACCOMPLISHMENTS• TOC&INTRO Ion Transport Through Porous Graphene ................................................................................................................118 Katelyn Conrad, Biomedical Engineering, Arizona State University . . . . . .NNIN REU Site: University of Colorado, Boulder Nanocharacterization of Wood Fibers in Cement....................................................................................................120 Christopher Florencio-Aleman, Materials Science and Engineering, Columbia University . . NNIN REU Site: Georgia Tech Determination of Strength Degradation Mechanisms of Native Oxide on Silicon Nanostructures.............................122 Rafael Jesus Haro, Mechanical Engineering, University of Arizona . . . . . . . . . . NNIN REU Site: Cornell University The Effects of Lanthanum-Doping on Strontium-Titanate Thin Films Grown on Si <001> Substrates ........................124 Christine Karako, Chemistry, University of Dallas . . . . . . NNIN REU Site: NASCENT, The University of Texas at Austin Developing Bioinspired Slippery Coating on Industrial Steels .................................................................................126 Keiko Kato, Materials Science and Engr., University of Illinois at Urbana-Champaign . . . NNIN REU Site: Penn State University The Effect of Surface Roughness on Chemical Vapor Deposition of Hexagonal Boron Nitride..................................128 Daniel David Kuddes, Physics, University of Texas at Dallas . . NNIN REU Site: NASCENT, The University of Texas at Austin Thermodynamic Control of Lead Content in the Piezoelectric Thin Film....................................................................130 Fumiya Kurokawa, Mechanical Engineering, Kobe University, Japan . . . .NNIN iREG Site: The Pennsylvania State University Improvement of Lithium Ion Batteries with Selected Dopants..................................................................................132 Deanna Lanigan, Materials Science and Engr., University of Wisconsin . . .NNIN REU Site: Washington University in St. Louis Preparation of Transparent Conducting Copper Aluminum Oxide Films...................................................................134 Jeremy Leshin, Chemical Engineering, University of Florida . . . . . . . .NNIN REU Site: Washington University in St. Louis Challenges for Diamond Integrated Circuits ............................................................................................................136 Clay T. Long, Physics, The Pennsylvania State University . . . . . . . . . . . . . . . . . NNIN iREU Site: NIMS, Japan Mobility of the Two-Dimensional-Electron-Gas in Lattice-Matched InAlN/GaN Grown by Ammonia MBE....................138 Frank John Luciano, IV, Material Science and Engineering, University of Florida . . . . NNIN REU Site: UC Santa Barbara Electro-Mechanical Characterization of Gold Nanowire Meshes ..............................................................................140 Connor G. McMahan, Mechanical Engineering, Massachusetts Institute of Technology NNIN REU Site: University of Colorado Growth of Molybdenum Disulfide Atomic Layers....................................................................................................142 Brendan McMurtray, Chemical Engineering, University of Maryland, Baltimore County . . NNIN REU Site: Howard University Growth and Characterization of Synthetic Diamond...............................................................................................144 Veronica Medrano, Electrical Engineering, Texas A&M University . . . . . . . . . .NNIN REU Site: Howard University •2013•NNIN•REU•RESEARCH•ACCOMPLISHMENTS• vii TOC&INTRO High Strain Low Voltage Induced Densified Vertically Aligned Carbon Nanotube Ionic Actuators.............................146 Joshua Michalenko, Electrical Engineering, New Mexico State University NNIN REU Site: The Pennsylvania State University Carbon Coated Tin-Seeded Silicon Nanowires for Lithium-Ion Battery Anodes .........................................................148 Daichi Oka, Chemistry, The University of Tokyo, Tokyo, Japan . . . . . . . NNIN iREG Site: The University of Texas at Austin Advanced Synthesis and Nano-Characterization of Graphene on Platinum <111> Substrates ....................................150 Stephen Olson, Applied Physics, Bethel University; EE, University of Minnesota . . . . . . . NNIN iREU Site: NIMS, Japan Study of the Electron Blocking Layer in Gallium Nitride Devices ..............................................................................152 Eric Reichwein, Physics, University of California Santa Cruz . . . . .NNIN REU Site: University of California, Santa Barbara Hydrogen as a Potential Cause for Native n-type Conductivity in Tin Dioxide...........................................................154 Emily M. Ross, Engineering, Harvey Mudd College . . . . . . . . . . . . . . . . . . . NNIN iREU Site: NIMS, Japan Solid-State NMR of (CdSe) (Propylamine) ...........................................................................................................156 13 13 Michael West, Chemical Engineering and Physics, University of Arkansas . .NNIN REU Site: Washington University in St. Louis Synthesis of Metal Supported Catalysts for the Hydrogenolysis of Lignin..............................................................158 Jeanne Xu, Chemistry, Wellesley College . . . . . . . . . . . . . . . .NNIN REU Site: Washington University in St. Louis Fabrication of Smart Gels with Tunable Stiffness ...................................................................................................160 Carolyn Zhang, Biochemistry and Cell Biology, University of California San Diego . . . . NNIN REU Site: Harvard University Mechanical Devices, pages 162-169 Design of a Microfluidic Device to Measure the Deformability of Cancer Cells .................. 162 Gabriel R. López Marcial, Mechanical Engineering, Puerto Rico . . NNIN REU Site: Cornell University Designing Directional Micro-Machined Microphones.......... 164 Alexandro Rocha, Jr., Applied Science, NW Vista College . . . . . . NNIN REU Site: Univ. of Texas at Austin Studying the Interfacial Dynamics of Miscible Systems with Microfluidics..............................................................166 John Schwalbe, Chemical and Biomolecular Engr, Cornell University . . . . . . . NNIN REU Site: University of Washington Full-Body Silicon Medical Tweezers for Cancerous Tissue Detection and Characterization .......................................168 Connie Wu, Electrical Engineering and Finance, University of Pennsylvania . . . . . . . . NNIN REU Site: Cornell University viii •2013•NNIN•REU•RESEARCH•ACCOMPLISHMENTS•

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Chromium-Doped Particles: Deanna nanotechnology, under the guidance of their mentor. devices were used to confirm the gold plating conditions. automatically through the operating program and manually. The exposed aluminum was then anodized in a solution We used an Arduino.

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