Table Of Contentइंटरनेट मानक
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timely dissemination of this information in an accurate manner to the public.
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“The Right to Information, The Right to Live” “Step Out From the Old to the New”
IS 13403 (1992): Pesticide - Anilophos EC [FAD 1:
Pesticides and Pesticides Residue Analysis]
“!ान $ एक न’ भारत का +नम-ण”
Satyanarayan Gangaram Pitroda
““IInnvveenntt aa NNeeww IInnddiiaa UUssiinngg KKnnoowwlleeddggee””
“!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता हहहहै””ै”
Bhartṛhari—Nītiśatakam
“Knowledge is such a treasure which cannot be stolen”
IS 13403: 1992"·
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Indian Standard
PESTICIDE -- ANILOPHOSEC~
SPECIFICATIO·N
UDC 632-951 ANI
:}o
.'.'-\
s,»
<0 DIS 1992
BUREAU OF INDIAN STANDARDS
MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI 110002
May 1992 Price Group 1
AMENDMENT NO.1 JULY 1993
TO
IS13403: 1"2 PESTICIDE- ANILOPHOS EC
SPECIFICATION
c.....
(P.,e1, 3.2.1)- SubstitutetilefoUowiDgfortheexistingmatter:
'3.Z.1 DacriptiIM
'I1Ie malCriallbaU beia 1beformof. liable liquid. Sometulbidity/s.peDded
_lIerDIIy bep-. It Mall readllyform I.emulsioDondilutioDwithwlter
IUilibieforIplly.·
('ADO!)
AMENDMENT NO. 2 JULY 1994
TO
IS 13403: 1992 PESTICIDE-ANILOPHOS EC
SPECIFICATION
(Page 1,clause 3.%.5 )- Delete.
(FAD1)
ReproaraphyUBit,BIS,NewDelhi,IDdia
Pesticides Sectional Committee, FAD 1
FOREWORD
This Indian Standard wasadopted bythe Bureauof Indian Standards, after the draft finalized by
the Pesticides Sectional Committee had been approved by the Food and Agriculture Division
Council.
Anilophos ECisgenerallyusedas a herbicide.
Anilophos EC isgenerallymanufactured to contain 30 percent (mlm )ofanilophos.
In the preparation of this standard, due consideration has been given to the provisrons of the
Insecticides Act, 1968 and the Rulesframedthereunder. However,this standard is subject to the
restrictionsimposedunder the Actand Rules, whereverapplicable.
For the purpose of decidingwhethera particular requirement of this standard iscompliedwith, the
finalvalue, observedor calculated, expressingthe result of a test or analysis, shall be rounded off
in accordancewith IS 2: 1960'Rules for rounding offnumerical values (revised)'. The number
of significantplacesretained in the rounded offvalueshould be the same as that of the specified
valuein this standard.
•
IS 13413: 1992
Indian Standard
PESTICIDE - ANILOPHOS EC
SPECIFICATION
1 SC..P. PI: 3.2.3 Flash Point (Abel)
This standard prescribes therequirements and the When determined by the method prescribed in
naethodsof sampliDI and testfor anilophosEe. IS 1448 [P : 20] : 1982, the flash point of the
materialshall beabove24SoC.
2 RUEIlENCES
3.1.4 Emulsion Stability
The IndianStandards listed below are necessary Anyseparationincludingcreamingat the top and
adjunctsto thisstandard: sedimentation at the bottom of 100 ml of
emulsionprepared in standard hard water with
IS No. T;t/~ 2·0 ml of Be, shall not exceed 2°0 ml when
tested by the method prescribed in 13.3 of
1070 : 1977 Waterforgenerallaboratory use
IS 6940 : 1982.
(secondreYislon )
1448 Methodsof test for determina 3.2.5 HeatSlability
[P:20]: tion of flash point by Abel
1982 apparatus (first revision) The materialafter being treated by the method
prescribed in 13.4ofIS 6940: 1982 shall comply
6940: 1982 Methods of test for pesticides with the requirementsliven in 3.2.1 to 3.2.4, 3.3.1
and their formulations (first and 3.3.2of thisstandard.
revision)
NOTE- The material need not be put to heat
8190 Requirements for packing of stabilitytestafter the expiry of half of its shelf-hfe,
( Part 2) : pesticides: Part 2 Liquid pesti as ascertained from the dates of manufacture and
1988 cides(second revision) expirydeclared on thecontainer.
10627 : 1983 Method of sampling of pesti- 3.3 Cbemical
eida! formulations
3.3.1 Anilophos Content
13402 : 1992 Anilophos,technical
When determined by the method prescribed in
3 REQUIREMENTS Annex B of IS 13402 : 1992 the observed
anilophoscontent ( m/m) ofany of the samples
shall not differ from the declared nominal value
3.1 COD.tltuentl
bymore than the tolerancelimits givenbelow:
3.1.1 The material shall consist of anilophos, Nomina/ Value, Percent Tolerance Limits,
technicaldissolved in suitable solventts) together Percent
withemulsifying agent(s) and with or without
stabilizer(s) and/or couplers. Up109 +101 ofthe
-5 I
±S
~ nominal
3.1.2 Anilophostechnical, employed in the manu Above9andbelowSO
I value
facture of the material, shall conform to
+S
IS 13402 : 1992. SO and above JI
-3
3.2 PIiJaleal
3.3.1 Acidity/Alkalinity
3.2.1 Delcription Whentestedbythe methodprescribed in 13.5 of
IS 6940 : 1982, the acidity (as H.SO.) or
The materialshallbe a clear, homogeneous and alkalinity(as NaOH) of the material shall be
stable liquid,freefromsedimentand/or suspended not more than 0'3 and 0·2 percent by mass
matter. It shall readily form an emulsion on r~spectively.
dilutionwithwater,suitableforspray.
4 PACKING
3.3.2 ColdTeJI
The material sball be packed in rectangular/
No turbidity or separationoflolidor oily matter round tinplate containers. 4-litres quantity of
sballoccur When the material is subjected to the the material shall be packed in round tin
cOld telt at IO·e u prescribed in 13.1 of containcr.shallbefurther packed in corrugated
IS 6940 : 1982. flbro"'board boxes.
1
IS 13403: 1m
S MARKING 7 TESTS
man
5.1 Thecontainersshall be securely closed and 7.1 Test. becarriedout by the appropriate
shall bear legibly and indelibly tbe follo"ina method. referred to in3.21Dd3.3.
in addition to any other information as is
necessary under the Insecticide, Act. 1968 and 7.2 Weilh 7S0 rna of lample iato a 50-ml
Rulesframed thereunder: volumetricflast and make up tbe volume with
the mobile pbase. Mix well. Take out 10ml
a) Nameof thematerial; of thosolutionwitha pipetteinto anotber 5Q-ml
b) Indicationofthesourceofmanufacture; volumetric flask and add 10 ml of internal
standard solution, mix well and make up tbe
c) Batch number;
volume withthemobile phase. Alain mix well.
d) Dateofmanufacture; Theconcentrationof anilophos Ihall be around
e) Dateofexpiry; 0-9malml. DetermineanilophOicOlltent by the
hiBb performanceliquid chromatolrapby method
f) Netmaslofcontents;
described in A-2 of IS 13402: 1992.
s>
Nominalanilopholcontent,percent(mlm);
and
7.3 Weiah 360rna of the sample into a 2S-ml
b) A cautionary notice worded as in the volumetric flask. add 10ml of internal standard
Insect;cld,s Act, 1968 and Rules. solutionandmake up the volume with toluene
to the mark. Mix well. The concentration of
anilophosshallbearound4'3 malml. Determine
6 SAMPLING
theanilopbOicontentbythe g8S chromat08rapby
'.1 methoddescribedinA-3 ofIS 13402 : 1992.
Representative samplesofthematerialshallbe
drawn as prescribed in IS 10627: 1983 and
7.4 QualityofRealfDt.
testedwithin90day. ofit. manufacturing. When
thematerialisoffered forinspection after90 days
Unless specified otherwise, pure chemicals and
ofitsmanufacturing, sampling shall alsobedone
distilled water (see IS 1070: 1977) sball be
accordingto IS 10627: 1983. However. in the
employed intests.
latter case the criteria for conformity of the
material when tested, shall be the limits of
NOTE - "ureChemicals'shall mean chemicals that
tolerances, as applicable over the declared
do notcontainimpurities,which affect the results of
nominalvalueandgiven in thisstandard. analysis.
2
Staadard Mark
The useof the Standard Mark isgoverned by the provisions ot' the Bur~au of Indian
StandardsAct, /986 and tho Rulesand Regulations made thereunder. The Standard Mark on
products covered byan Indian Standard conveys the assurance that they have been produced
to comply with the requirements of that standard under a well defined system of inspection,
testing and quality control which is devised and .supervised by BISand operated bythe
producer. Standard marked products are also 'ccntinuouslychecked by BISfor conformity
to that standard as a further safeguard. Details of conditions under which a licence for tbe
uee of the Standard Mark may begranted to manufacturers or producers Dlay beobtained
from the Bureauof Indian Standardl.
