FTIR and UV-Vis Accessories and Supplies - Hellma Analytics

167 Pages·2012·10.3 MB·English

C O M P R E H E N S I V E C A T A L O G O F
FTIR and UV-Vis
Accessories and Supplies
MIRacle™
The Most Universal ATR
WWW.PIKETECH.COM
The PIKE Technologies team looks
forward to helping you with our
spectroscopy sampling accessories
and thanks you for your business.
We are PIKE Technologies, an innovative company growing consistently over our
20 years and focused upon serving customers with their FTIR and spectroscopy
applications. We are always looking for new ways to help make your spectroscopy
sampling easier and more effective. We think you will see in our new products
introduced each year that you, our customers, have helped us to achieve this goal.
If you do not see what you need in this catalog, please contact us. Your input
may become one of our product offerings in the future. We look forward to
serving you with our products and support.
A unique enterprise specializing in the imaginative
design and creation of excellent spectroscopic accessories,
providing high quality solutions to all customers.
6125 Cottonwood Drive
Madison, WI 53719
[phone]
[phone] (FAX)
[email protected]
WWW.PIKETECH.COM
FTIR INSTRUMENT CODE XX
ABB Bomem
FTLA2000-100 (Arid Zone). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 80
Michelson 100, MB Series. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 81
MB 3000 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 82
Analect/Hamilton Sundstrand
Diamond 20 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60
Bruker Optics
IFS™, Vector™, Equinox™ Series . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50
Tensor™, Vertex™ with recognition (Quick-Lock) . . . . . . . . . . . . . . . . . . . . . . . . 51
Buck Scientific
M500. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65
Digilab/Bio-Rad/Varian/Agilent
Excalibur™, Scimitar™, FTS, 600-IR Series Cary 600/6000 Series . . . . . . . . . . . . 10
Excalibur, Scimitar, 600-IR Series Cary 600/6000 Series with recognition . . . . . 13
Horiba
7000 Series . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
Interspectrum
Interspec 200-X. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 90
Jasco
300/600 Series. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 56
400. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 57
4000/6000 Series. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58
4000/6000 Series with recognition. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
JEOL
Winspec™ Series . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
Lumex
InfraLUM® FT-02, FT-08. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 67
Midac
M Series. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
ORIEL. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 95
PerkinElmer
1700 Series . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 70
Spectrum™ GX, 2000. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71
Spectrum BX/RX, 1600, Paragon 1000 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73
Spectrum ONE, 65, 100, 400, FRONTIER. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74
Spectrum TWO. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75
Shimadzu
8300, 8400 Series, IRPrestige, IRAffinity. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
IRPrestige, IRAffinity with recognition (QuickStart) . . . . . . . . . . . . . . . . . . . . . . 16
Thermo Fisher Scientific/Nicolet/Mattson
Infinity, Galaxy, RS Series. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Genesys™, Satellite, IR 300 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
Impact™ 400, Magna-IR™, Protégé™, 500/700 Series, Avatar™,
Nexus™, Nicolet™ Series, Nicolet iS™10, Nicolet iS™50 . . . . . . . . . . . . . . . . . . . 40
Nicolet iS™5. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42
Please contact PIKE for UV-Vis instrument codes
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TABLE OF CONTENTS
Sampling Kits – If You Don’t Know Where to Start
Products Overview.......................................................................................... 1
Pages 1–6 Standard Transmission Sampling Kit (STS)...................................................... 2
Comprehensive Transmission Sampling Kit (CTS)........................................... 3
Educational Transmission Sampling Kit (ETS)................................................. 4
Valu-Line Kit.................................................................................................... 5
Ultima Sampling Kit........................................................................................ 6
Attenuated Total Reflectance –Liquids, Solids and In-Between
Products Overview.......................................................................................... 7
Pages 7–32 MIRacle – Fast and Easy IR Sampling.............................................................. 8
GladiATR – Highest Performance Diamond ATR.............................................. 12
GladiATR Vision – Diamond ATR with Sample View........................................ 14
Dedicated GladiATR and GladiATR Vision Sampling Tools –
More Options to Address Your Specific Application Requirements............ 16
Multiple Reflection HATR –
Maximum Sensitivity and Highly Versatile FTIR Sampling........................ 17
ATRMax II Variable Angle Horizontal ATR Accessory –
HATR for Inquisitive Minds....................................................................... 21
VeeMAX III with ATR –
Variable Angle, Single Reflection ATR for Depth Profiling Studies............. 24
JetStream ATR Accessory –
Measurements of Liquids under Varying Conditions................................ 27
Classic VATR –
Variable Angle ATR for Analysis of Solids, Films and Coatings................. 28
Theory and Applications................................................................................. 29
Diffuse Reflectance – From Powders to Plastic Bumpers
Products Overview.......................................................................................... 33
Pages 33–42 EasiDiff – Workhorse Diffuse Reflectance Accessory......................................... 34
DiffusIR – Research Grade Diffuse Reflectance Accessory................................ 35
UpIR – Upward Looking Diffuse Reflectance Accessory.................................... 37
AutoDiff – Automated Diffuse Reflectance Sampling....................................... 38
X, Y Autosampler – Transmission and Reflectance Automated
Sampling in Microplate Format................................................................. 39
Sample Preparation and Loading Kit –
The Easiest Way to Work With Powder Samples....................................... 40
Abrasion Sampling Kit..................................................................................... 40
Theory and Applications................................................................................. 41
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TABLE OF CONTENTS
P
I
K
E
T Specular Reflectance – Thin Films and More
E
C
H Products Overview.......................................................................................... 43
N
O Pages 43–52 VeeMAX III – The Ultimate Variable Angle Specular Reflectance Accessory....... 44
L
O 30Spec and 45Spec –Specular Reflectance for Thick Films............................. 46
G
I
E 80Spec – Grazing Angle Specular Reflectance for Thin Films........................... 47
S
AGA – Advanced Grazing Angle Specular Reflectance for Thin Films
with Precise Spot Control............................................................................ 48
W
10Spec – Near-normal Sample Reflectivity Measurements.............................. 49
W
W
Absolute Reflectance Accessory – Measure Absolute Sample Reflectivity........ 50
.
P
I Theory and Applications................................................................................. 51
K
E
T
E
C
H
.C Polarization – For Oriented Samples and Research Applications
O
M Products Overview.......................................................................................... 53
Pages 53–56 Polarizers – Manual and Automated Versions for Molecular Spectroscopy..... 54
6 Theory and Applications................................................................................. 55
0
8
-
2
7
4
- Integrating Spheres – Reflectance From All Perspectives
2
7
2 Products Overview.......................................................................................... 57
1
Pages 57–64 Mid-IR IntegratIR – Integrating Sphere............................................................ 58
NIR IntegratIR – Integrating Sphere................................................................ 60
Introduction and Theory................................................................................. 62
Remote Sampling Accessories –
Extending Your Sample Compartment
Pages 65–70 Products Overview.......................................................................................... 65
FlexIR – Hollow Waveguide Accessory for Remote Infrared Sampling............. 66
FlexIR –
NIR Fiber Optic Accessory for Fast and Remote Sample Identification...... 68
Heated Liquid Sample Holder –
Characterization of Liquids at Controlled Temperatures........................... 69
Microsampling Products – From Microns to Millimeters
Products Overview.......................................................................................... 71
Pages 71–80 µMAX – Sample Compartment Microscope for FTIR........................................ 72
Compact Transmission/Reflection S84 Microscope Heat Stage –
High Temp Measurements under Vacuum or Controlled Gas Flow........... 75
Microsampling Tools – Compression Cells and Sample Manipulation............ 76
Micro Diamond Cell – For Compressing and Holding Samples for Microanalysis... 77
Beam Condensers – 4X and 6X Versions for FTIR........................................... 78
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Transmission Sampling – Automated & Manual Technologies
Products Overview.......................................................................................... 81
Pages 81–114 Transmission Multi-SamplIR – Automated In-Sample Compartment Accessory.... 82
RotatIR – Automated Rotating Sample Stage................................................... 83
Automated Horizontal Transmission Accessories – For Films or Pellets......... 84
X, Y Autosampler –
Transmission and Reflection, Automated Sampling in Microplate Format....... 85
Liquid Samples
Press-On Demountable Cell – For Viscous Liquids and Mulls......................... 86
Demountable Liquid Cells – For Versatile Pathlength Liquid Sampling.......... 87
Super-Sealed Liquid Cells – For Precision, Fixed Pathlength Liquid Sampling.... 88
Long-Path Quartz Liquid Cells –
For Analysis of Hydrocarbon Content and Related Measurements................ 89
Falcon Mid-IR Transmission Accessory –
For Precise Temperature Control of Demountable Liquid Cells................ 90
Falcon NIR Transmission Accessory – Quantitative and Qualitative
Analysis of Liquids under Precise Temperature Control............................ 92
Cryostat190 – Ultralow Temperature Accessory for Liquid and Solid
Transmission Sampling............................................................................. 93
Solid Samples
Cryostat190 – Ultralow Temperature Accessory for Liquid and Solid
Transmission Sampling............................................................................. 93
Heated Solid Transmission Accessory –
Measurements of Optical Components and Polymers.............................. 94
Bolt Press & Hydraulic Die – Low-Cost Pellet Preparation.............................. 95
Hand Press – For Making Smaller Pellets........................................................ 95
Evacuable Pellet Press – For Preparation of High Quality Pellets.................. 96
Heated Platens Accessory – For Making Thin Films of Polymeric Samples
for Transmission FTIR Analysis................................................................. 97
CrushIR – Digital Hydraulic Press.................................................................... 98
Auto-CrushIR – Programmable Hydraulic Press............................................... 99
ShakIR and Super ShakIR – For Optimized Sample Mixing............................. 100
Sample Preparation Accessories – For Solid Material Analysis....................... 101
Optical and Sampling Components, Polishing Kits
Sample Holders – For Transmission FTIR Analysis of Pellets and Films.......... 102
Disks, Windows and Powders –
For Transmission FTIR Analysis of Solid and Liquid Samples..................... 103
Crystal Polishing Kit – Extending the Life of IR Transparent Windows............ 106
Gas Samples
Short-Path Gas Cells – For Samples with Higher Vapor Phase Concentration..... 107
Heated Gas Flow Cell –For Streaming Gas Analysis........................................ 108
Long-Path Gas Cells –
For Measurement of Low Concentration Vapor Components................... 109
Theory and Applications................................................................................. 111
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TABLE OF CONTENTS
P
I
K
E
T Special Applications
E
C
H Products Overview.......................................................................................... 115
N
O Pages 115–126 Vertical Wafer Accessory – For Analysis of Semiconductor Wafers.................. 116
L
O MappIR and MAP300 – For Automated Analysis of Semiconductor Wafers.... 117
G
I
E TGA/FTIR Accessory – Identification and Quantification of Evolved Gases
S
from Thermogravimetric Analyzer............................................................ 119
GC-FTIR Accessory –
W Combining GC Separation with Identification Power of FTIR................... 121
W
W External Sample Module – Extending Sampling Efficiency.............................. 122
.
P PA301 and PA101 – Photoacoustic Accessory for Analysis of
I
K
Difficult Samples and Depth Profiling...................................................... 123
E
T
E Semiconductor Applications – FTIR Sampling Techniques Overview.............. 125
C
H
.
C
O
M
UV-Vis Accessories
Products Overview.......................................................................................... 127
6
0 Pages127–138 UV-Vis Cuvettes, Cells, Vials and Holders........................................................ 128
8
-2 UV-Vis Polarizers –Manual and Automated Versions..................................... 130
7
4 UV-Vis Spec – Slide Mounted Specular Reflectance Accessories....................... 131
-
2 UV-VIS 85Spec – Specular Reflectance Accessory............................................. 132
7
2 UV-Vis VeeMAX – Variable Angle Specular Reflectance Accessory.................... 133
1
Falcon UV-VIS – Precise Cell Temperature Control Accessory........................... 134
Peltier-Controlled Cuvette Holders for UV-Vis Spectrophotometers –
Experiments Under Tightly Controlled Temperature Conditions............... 135
Out-of-Compartment Microplate Reader –
Plate Reading Option for UV-Vis Spectrophotometers.............................. 136
Automated XY, R-Theta and Y-rotation Stages for
UV-Vis Spectrophotometers..................................................................... 137
Standards, Software and Databases
Products Overview.......................................................................................... 139
Pages139–145 Reference Standards –For Calibrating FTIR Spectrometers............................ 140
PIKECalc Software –For FTIR Sampling Computations................................... 143
ATR Spectral Databases – Optimize Search Results for ATR Spectral Data...... 144
Transmission Spectral Databases –
High Quality Spectral Data for Optimized Search Results.......................... 145
Index
Catalog Index – Alphabetical........................................................................... 146
Catalog Index – Part Number.......................................................................... 149
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Sampling Kits
If you are not sure where to start, check out these
PIKE Technologies sampling kits. You will immediately
find everything you need for the most basic FTIR
experiments, and you will be able to collect your
first spectrum in less than 30 minutes from the
time the kit arrives.
One of the goals of PIKE Technologies is to
make the life of an applications chemist easier. FTIR
spectroscopy can be confusing when it comes to
sampling techniques, sampling accessories and all
the little gadgets required to successfully prepare
the sample for analysis – especially if you want to
obtain good spectra. For this reason, the first few
pages of this catalog are fully dedicated to sampling
kits. We hope that this approach will give you a head
start and remove confusion when selecting accessories
for your applications, especially when you are a
first time user. The kits are carefully designedto
include all necessary components. Theyeliminate
guesswork and assure that you have everything you
need for immediate productivity.
Standard Transmission Sampling Kit
Everything you need to run liquid
Page 2
and solid samples by transmission
IR spectroscopy
Comprehensive
Transmission Sampling Kit
Page 3
Complete gas, liquid
and solid sampling
Educational Transmission
Sampling Kit
Page 4 An economical assembly
of FTIR sampling tools for
transmission sampling
Valu-Line Kit
High performance set of modern
Page 5
FTIR accessories addressing all
solid and liquid sampling needs
Ultima Sampling Kit
With the highest performance,
Page 6
single-reflection ATR and backup
accessories to do it all!
01_Sampling 12-12-12_01_Sampling 12/13/12 1:12 PM Page 2
P Standard Transmission Sampling Kit (STS) – Everything You Need
I
K
E to Run Liquid and Solid Samples by Transmission IR Spectroscopy
T
E
C
H This general purpose kit contains tools and materials for liquid
N and solid sampling. A demountable cell (drilled and undrilled
O
L windows with precision Teflon spacers, plus 2" x 3"standard cell
O
holder) is provided for measurements of liquid samples. Viscous
G
I liquids can be measured directly as a thin film between the KBr
E
S windows. The kit includes a hand operated press for the preparation
of 7 mm KBr pellets. A mortar with pestle and Nujol™/Fluorolube®
are provided for mull making – another popular method for
W preparation of solid samples. In addition, the kit contains a set of
W
the most popular sample holders including:universal holder for
W
. polymer films, KBr pellet holder and PIKE disposable/storage
P
I cardboard cards for pellets and polymer films. For a complete
K
product listing, please refer to the table below.
E
T
E
C
H ORDERING INFORMATION
.
C
O PART NUMBER DESCRIPTION
M
162-1000 Standard Transmission Sampling Kit (STS) – Solids and Liquids
Includes: Sample preparation tools, mull liquids, cells, windows
and cell holders required for preparation and analysis of solid
6 and liquid samples
0
8
-2 Included Parts and Materials
7 PART NUMBER DESCRIPTION
4
- 160-8010 KBr Powder, 100 g
2
7 161-0510 Fluorolube, 1 oz
2
1 161-0500 Nujol, 1 oz
FEATURES OF THE STANDARD 042-3035 Spatula – Spoon
TRANSMISSION SAMPLING KIT 042-3050 Spatula – Flat
•Complete kit for transmission FTIR sampling 161-5050 Mortar and Pestle, 50 mm
•Make KBr pellets and mulls for solid samples 161-1027 PIKE Hand Press (for KBr Pellets)
•Run liquid samples for qualitative and quantitative analysis 161-1010 7 mm Die Set
161-1018 KBr Pellet Holder
161-6000 Finger Cots (12 pcs)
162-1100 Demountable Liquid Cell Assembly
160-1015 Window, KBr 32 x 3 mm, Drilled (6 ea.)
160-1010 Window, KBr 32 x 3 mm, Plain (6 ea.)
162-1290 Teflon® Spacers – Assortment
161-0521 Syringe, 2 mL (2 ea. in kit)
162-3610 Press-On Demountable Liquid Cell Holder for 32 mm Windows
162-5600 Universal Sample Holder*
162-5300 Magnetic Film Holder – for 13 mm pellets and film samples
162-5400 Film Sampling Card – 20 mm clear aperture, 10 each*
*Note: Cell holders marked “*” fit all standard slide mounts, but due to their
height may not allow for a complete sample compartment door closure on some
smaller spectrometers. Please consult PIKE Technologies before placing an order.
2
01_Sampling 12-12-12_01_Sampling 12/13/12 1:12 PM Page 3
Comprehensive Transmission Sampling Kit (CTS) – S
A
Complete Gas, Liquid and Solid Sampling M
P
L
The CTS Kit includes a 100 mm long, 38 mm diameter gas cell, I
in addition to all the sample preparation and mounting tools N
described in the STS Kit on the previous page. The cell body is G
made of Pyrex® glass and features straight-tube inlet and outlet
K
ports with stopcocks. The gas cell comes with all necessary
gaskets, two KBr windows and slide-mounted cell holder, and I
T
is designed for gas measurements at ambient temperature and S
normal atmospheric pressure.
–

I
ORDERING INFORMATION F
PART NUMBER DESCRIPTION Y
162-2000 Comprehensive Transmission Sampling Kit (CTS) – O
Gases, Solids and Liquids U
Includes: Sample preparation tools, mull liquids, cells,
windows and cell holders required for preparation and D
analysis of gas, solid and liquid samples O
N
Included Parts and Materials
’
PART NUMBER DESCRIPTION T
160-8010 KBr Powder, 100 g K
161-0510 Fluorolube, 1 oz N
161-0500 Nujol, 1 oz O
W
042-3035 Spatula – Spoon
042-3050 Spatula – Flat W
161-5050 Mortar and Pestle, 50 mm H
161-1027 PIKE Hand Press (for KBr Pellets) E
R
FEATURES OF THE COMPREHENSIVE 161-1010 7 mm Die Set
E
TRANSMISSION SAMPLING KIT 161-1018 KBr Pellet Holder
T
•Complete sampling kit for analysis of solids, liquids 161-6000 Finger Cots (12 ea.) O
and gas samples by transmission 162-5300 Magnetic Film Holder – for 13 mm pellets and film samples
S
•Make KBr pellets and mulls for solid samples 162-1100 Demountable Liquid Cell Assembly T
•Run qualitative and quantitative analysis of liquid samples 160-1015 Window, KBr 32 x 3 mm, Drilled (6 ea.) A
R
•Identify and quantify gas samples 160-1010 Window, KBr 32 x 3 mm, Plain (6 ea.)
T
162-1290 Teflon® Spacers – Assortment
161-0521 Syringe, 2 mL (2 ea. in kit)
162-3610 Press-On Demountable Liquid Cell Holder for 32 mm Windows
162-5600 Universal Sample Holder*
162-2200 100 mm Gas Cell, 38 mm diameter
160-1320 Window, KBr 38 x 6 mm (2 ea. in kit)
162-5400 Film Sampling Card – 20 mm clear aperture, 10 each*
*Note: Cell holders marked “*” fit all standard slide mounts, but due to their
height may not allow for a complete sample compartment door closure on some
smaller spectrometers. Please consult PIKE Technologies before placing an order.
3