Advanced electron microscopy and nanomaterials : selected, peer reviewed papers from the First Joint Advanced Electron Microscopy School for Nanomaterials and the Workshop on Nanomaterials (AEM-NANOMAT '09), Saltillo (Coahuila) México, September 29th-Oct

147 Pages·2010·36.167 MB·English

by  Arturo Ponce, Darío Bueno

Advanced
Electron Microscopy
and Nanomaterials

Advanced Electron Microscopy
and Nanomaterials
Selected, peer reviewed papers from the First
Joint Advanced Electron Microscopy School for Nanomaterials
and the Workshop on Nanomaterials (AEM-NANOMAT’09),
Saltillo (Coahuila) México,
September 29th-October 2nd, 2009
Edited by:
Arturo Ponce and Darío Bueno

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Volume 644 of
Materials Science Forum
ISSN 0255-5476
Full text available online at http://www.scientific.net

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Saltillo (Coahuila) Mexico
th nd
September 29 – October 2 , 2009

Organizers
Local Committee:
Chairman Arturo Ponce Pedraza [email protected]

Co-Chairman Darío Bueno Baqués [email protected]

Program Coordinator: Leticia Rodríguez González [email protected]

Gerardo Martínez and Esmeralda [email protected]
School Secretariat:
Saucedo [email protected]

Support Committee: Oliverio Rodríguez Fernández [email protected]

Exhibition contact: Jesús Olivo Padilla [email protected]

Student Support
Luis Ernesto Elizalde Herrera [email protected]
Coordinator:
Treasurer: Josefina del Refugio Pérez Huerta [email protected]

National Committee:
Institute of Physics National University of
Jesús Arenas Alatorre [email protected]
Mexico

Juan Méndez-Nonell Research Center for Applied Chemistry (CIQA) [email protected]

Vicente Garibay Febles Mexican Petroleum Institute (Mexico) [email protected]

Leopoldo Enriquez Jeol de México SA de CV [email protected]

Fernando Mendoza FEI Company [email protected]

Kaheri Arellano Carl Zeiss de México, SA de CV [email protected]
Invited speakers
Dual/Beam (SEM/FIB) applications
Dr. Tomas Vystavel
FEI Specialist Title 1: TEM Sample Preparation with DualBeam
DUAL-BEAM (SEM/FIB) – Netherlands Title 2: Advanced DualBeam Applications in NanoPrototyping
and 3-D Characterization
High resolution transmission electron microscopy
(HRTEM) and scanning transmission electron
Dr. Dong Tang
microscopy (STEM)
FEI Specialist
HRTEM and STEM - Netherlands Title 1: Atomic scale high-resolution transmission electron
microscopy
Title 2: STEM applications in nano-sciences
In-lens and LAB detectors in FEG-STEM
M.C. Martin Palacios
Title 1: The high resolution at low kV in a FEG scanning
Jeol Specialist - Mexico
electron microscope
Title 2: Study of nonconductive samples using the r-Filter
Dr. Antonio Casares Advanced EELS and Omega filter for TEM
Carl Zeiss NTS GmbH Specialist applications
EELS and Omega filter – Germany
Title: Advanced EELS and Omega filter for TEM applications
Dr. Marco Antonio Ramirez Cross Beam (AURIGA)
Carl Zeiss
Cross Beam (AURIGA) – México Title: SEM/FIB preparation samples
Dr. Alfredo Gomez HRTEM and electron diffraction simulation
Institute of Physics UNAM
Mexico Title: HRTEM and electron diffraction simulation
kinematical and dynamical diffraction and HRTEM
Dr. Laurence D. Marks
Northwestern University – USA Title: kinematical and dynamical diffraction and HRTEM:
quantitative analysis
Dr. Stavros Nicolopoulos Precession Electron diffraction in TEM
NanoMEGAS SPRL – Belgium
Title: Precession interface Spinning Star
Dr. José Reyes-Gasga Electron diffraction
Institute of Physics UNAM
Mexico Title: Dynamical electron diffraction in crystals
Dr. Jean-Paul Morniroli LACBED. Applications in Materials Science
Laboratoire de Metallurgie Physique
CNRS – France Title: LACBED. Applications in Materials Science
Dr. Miguel Ávalos Borja EELS
CNyN-UNAM - Mexico
Title: EELS theory and applications
International Advisory Committee
Juan Méndez-Nonell CIQA - (Mexico)
Fernando Ponce Arizona State University (USA)
Miguel José Yacamán University of Texas at San Antonio (USA)
János L Lábár Institute for Technical Physics (Hungary)
Sven Hovmöller Stockholm University (Sweden)
David Ríos IPICYT (Mexico)
Robert Sinclair University of Stanford (USA)
Karla Balzuweit Universidade Federal de Minas Gerais (Brazil)
Rafael Garía Roja University of Cadiz (Spain)
José Reyes-Gasga National University of Mexico (Mexico)
Alejandro Zúñiga University of Chile (Chile)
Gustavo Martínez National University of Colombia (Colombia)
Walter Jose Botta Federal University of São Carlos (Brazil)
Jean-Paul Morniroli University of Lille (France)
Sergio Lozano-Perez University of Oxford (UK)

Topics

•Multifunctional nanocomposites
•Smart materials
•Nanoparticles: synthesis and applications
•Structure phenomena and modeling
•Growth of thin films
•Semiconductors and optoelectronic materials
•Other nanomaterials and interdisciplinary topics

Table of Contents
Organizers
Invited Speakers
International Advisory Committee
Picture
Topic 1: Multifunctional Nanocomposites
Precession Electron Diffraction Assisted Orientation Mapping in the Transmission Electron
Microscope
J. Portillo, E.F. Rauch, S. Nicolopoulos, M. Gemmi and D. Bultreys 1
TEM Characterization on the Nanocomposite Al 7075 and Silver Nanoparticles Synthesized
by Powder Metallurgy
R. Flores-Campos, R. Deaquino-Lara, J.M. Herrera-Ramírez, A. Ponce, I. Estrada-Guel, M. Miki-
Yoshida and R. Martínez-Sánchez 9
Synthesis of Plasticizer-Based Ferrofluid and its Use in the Preparation of Magnetic PVC
Nanocomposite
E. Servín-Hernández, O.S. Rodríguez-Fernández and L.A. García-Cerda 13
Effect of Type and Concentration of Ionomer Compatibilizer on the Hdpe/ Ionomer/ Clay
Nanocomposites Morphology
S. López-García, S. Sánchez-Valdés and L.F. Ramos de Valle 17
Elemental Analysis of a Heterogeneous Polymeric System by EDS: Detection of the
Compatibilizer Agent Containing Si Atoms and Silver Nano-Particles (AgNP´s) in High
Impact Polystyrene
F. Soriano, C. de Anda, G. Morales and A. Ponce 21
Dielectric Properties of PMMA-SiO Hybrid Films
2
M.D. Morales-Acosta, M.A. Quevedo-López, H.N. Alshareef, B.E. Gnade and R. Ramírez-Bon 25
Synthesis and Characterization of Magnetic Polyurethane Nanocomposite Foams
A. Cámara-Hinojosa, D. Bueno-Baqués, O.S. Rodríguez-Fernández and R.F. Ziolo 29
Topic 2: Smart Materials
Preparation of Electrospun Barium Titanate – Polyvinylidene Fluoride Piezoelectric
Membranes
V. Corral-Flores, J.J. Pérez-Herrera, E. Torres-Moye, J. Romero-García, D. Bueno-Baqués and
R.F. Ziolo 33
Topic 3: Nanoparticles: Synthesis and Applications
Preparation and Properties of CoFe O Synthesized by the Modified Citrate-Gel Method
2 4
E.M. Múzquiz-Ramos, D.A. Cortés-Hernández, O.A. Herrera-Romero and J.C. Escobedo-
Bocardo 39
Alumina-Copper Composites with High Fracture Toughness and Low Electrical Resistance
E. Rocha-Rangel and J.G. Miranda-Hernández 43
Obtaining NiHCF Nanoparticles Using a Reverse Micellar System
A. Gutiérrez Becerra, T. Vega Venegas, M. Bárcena Soto, N. Casillas and J.I. Escalante 47
Iron Oxide Nanoparticles Obtained from a Fe(II) - Chitosan Polymer Film
J.F. Luna Martínez, E. Reyes-Melo, V. González-González, A. Torres-Castro, C. Guerrero-
Salazar and S. Sepúlveda-Guzmán 51
Synthesis and Characterization of Branched Gold Nanoparticles
A. Mayoral, A. Vazquez-Duran, S.G. Heinze and M.J. Yacaman 57
Surface Modification of ZnO Nanoparticles
R. Betancourt-Galindo, M.L. Berlanga Duarte, B.A. Puente Urbina, O.S. Rodríguez-Fernández
and S. Sánchez-Valdés 61
Topographical Characterization of Electrodeposited Nickel Nanoparticles on an Indium Tin
Oxide on Glass Thin Film
G.T. Martinez, G. Zavala and M. Videa 65